Pharmaceutical Materials

Product Name

N-Methylcyclohexylamine

N-Multiple Names

Methylcyclohexylamine;

N-Cyclohexylmethylamine;

N-Methyl-Cyclohexanamine;

1-Methylcyclohexylamine;

Cyclohexanamine,N-Methyl-;

Cyclohexylamine, N-Methyl-;

Cyclohexyl-Methyl-Amine;

Methylcyclohexylamine;

Methylcyclohexylamine,[Corrosivelabel]; Methylcyclohexylamine,[Flammableliquidandcorrosivelabels]; 1-Methylcyclohexanamine;

N-Methylcyclohexanaminium

CAS No. 100-60-7

EC No. 202-869-3

MF No. C7H16N

MW No. 114.2081

It is used as an intermediate of medicine and dyes, and as an intermediate of medicine and dyes and used as the intermediate of bromhexamine hydrochloride.

Advantage of N-Methylcyclohexylamine CAS No. 100-60-7

It is miscible with various organic solvents and slightly soluble in water

Keep in dark place

Good effect in demand use

Names and Identifiers

Name	N-Methylcyclohexylamine
Synonyms	Methylcyclohexylamine Cyclohexylmethylamine N-Methylcyclohexylamine cyclohexyl-methyl-amine 1-methylcyclohexanamine 1-Methylcyclohexylamine N-METHYLCYCLOHEXYLAMINE N-Cyclohexylmethylamine N-methyl-Cyclohexanamine Cyclohexanamine,N-methyl- N-methylcyclohexanaminium Cyclohexylamine, N-methyl- methylcyclohexylamine,[corrosivelabel] methylcyclohexylamine,[flammableliquidandcorrosivelabels]
CAS	100-60-7
EINECS	202-869-3
InChI	InChI=1/C7H15N/c1-8-7-5-3-2-4-6-7/h7-8H,2-6H2,1H3/p+1

100-60-7 – Physico-chemical Properties

Molecular Formula	C7H15N
Molar Mass	113.2
Density	0.868 g/mL at 25 °C (lit.)
Melting Point	-9–7 °C (lit.)
Boling Point	149 °C (lit.)
Flash Point	85°F
Water Solubility	5.4 g/100 mL (20 ºC)
Solubility	54g/l
Vapor Presure	11 mm Hg ( 40 °C)
Vapor Density	4 (vs air)
Appearance	Liquid
Specific Gravity	0.855 (20/4℃)
Color	Clear colorless to yellow
BRN	1523664
pKa	11.03±0.20(Predicted)
PH	12 (10g/l, H2O, 20℃)
Storage Condition	Keep in dark place,Inert atmosphere,Room temperature
Sensitive	Air Sensitive
Explosive Limit	2.2-10.5%(V)
Refractive Index	n20/D 1.456(lit.)
Physical and Chemical Properties	Character: colorless transparent liquid. boiling point 147~151 ℃ relative density 0.868 refractive index 1.4456 flash point 29 ℃ solubility it is miscible with a variety of organic solvents and slightly soluble in water.
Use	Used as intermediates in pharmaceuticals and dyes

100-60-7 – Risk and Safety

Hazard Symbols	C – Corrosive
Risk Codes	R10 – Flammable R21/22 – Harmful in contact with skin and if swallowed. R35 – Causes severe burns R20/21/22 – Harmful by inhalation, in contact with skin and if swallowed.
Safety Description	S16 – Keep away from sources of ignition. S26 – In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S36/37/39 – Wear suitable protective clothing, gloves and eye/face protection. S45 – In case of accident or if you feel unwell, seek medical advice immediately (show the label whenever possible.)
UN IDs	UN 2734 8/PG 2
WGK Germany	1
RTECS	GX1529000
TSCA	Yes
HS Code	29213099
Hazard Note	Corrosive
Hazard Class	8
Packing Group	II

Reference Information

Use

used as intermediate of medicine and dye intermediate of medicine and dye. Used as an intermediate for the drug bromohexylamine hydrochloride.

production method

1. Cyclohexylamine as raw material. Derived from the reaction of cyclohexanone with methylamine. The aluminum sheet was immersed in methanol, and then the high mercury chloride was added. The immersion was continued for 2H, and the temperature was not more than 55 ° C., and the soaking solution was removed. Ethanol was added to the above activated aluminum sheet, and a mixed solution of methylamine and cyclohexanone was added dropwise with stirring, and the mixture was heated to reflux and left overnight. 10% sodium hydroxide solution was added for alkalization, and the mixture was extracted twice with benzene, washed with water, and then distilled to recover benzene, and then N-methylcyclohexylamine was distilled off. The yield was about 80%.

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